Preparation of a fluorescent compound using pressure tubes.
Some reactions require strictly inert conditions avoiding the presence of oxygen or moisture. To keep water and oxygen away from the reaction mixture a method could be to keep things closed and this could be easily performed using pressure tubes or bomb tubes. Here we prepared everything under nitrogen atmosphere, the teflon valve was locked and the reaction was performed in a fume hood, just in any other case.
In the pressure tube on the left side there is a broken Pasteur pipette, that looks funny, but luckily doesn’t effect the reaction at all.













