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The PXRF is really just a very sophisticated vibe check
Two new trace element analyses have taken a fresh look at obsidian mirrors crafted by Inca and Aztec artisans.
Two new trace element analyses have taken a fresh look at obsidian mirrors crafted by Inca and Aztec artisans. Obsidian was most often used by peoples around the world to make flaked stone tools such as prismatic blades and arrow heads, yet with special care the glassy material can also be polished smooth to create remarkable objects. To stare into the depths of a polished obsidian mirror, is to step into a world of inky black reflections that seems to never end. This shadowy world has spurred centuries of speculation and occult fascination surrounding pre-Columbian obsidian mirrors. At long last, material scientists are shining some light into that world.
In the most recent issue of the journal Latin American Antiquity, Thomas Colligaro and his colleagues published a paper on their study of an alleged Inca obsidian mirror in the collections of the Muséum National d’Histoire Naturelle in Paris. It had long been presumed that this mirror was part of a shipment of spoils sent from Mexico to the Emperor Charles V of Spain by the conquistador Hernán Cortez, which was then intercepted by a French privateer. A thorough document review by the researchers, however, suggested that the mirror may instead have been collected by a French expedition to Ecuador in the mid-18th century.
To confirm their documentary findings, the researchers carried out a particle induced X-ray emission (PIXE) analysis of the mirror in order to identify trace elements found in the object’s mineral structure. By comparing the trace elements found in the mirror with the characteristics of known obsidian sources, the researchers attempted to trace where the original raw material had been collected. With the presence of small amounts of manganese, rubidium, and zirconium found in the Muséum National d’Histoire Naturelle’s mirror, Colligaro and his colleagues were able to rule out all known Mexican sources of obsidian. Instead, the composition of the mirror more closely resembled two obsidian deposits found in Ecuador.
PIXE analysis of the obsidian mirror held by the Muséum National d’Histoire Naturelle (No. 176.101).
Thus, the combined documentary evidence and trace element analysis strongly suggest that the object originated in Ecuador. Whether or not it was ever associated with the Inca empire, is more difficult to say. An 18th century note accompanying the mirror stated that it had been found “in the tombs of the Incas in Peru,” but by the time the mirror was collected by the French expedition, the Inca empire had long since dissolved in the face of European epidemic diseases and colonial occupation.
Just me and the pXRF machine this morning, running our tests, looking for those sweet matching elemental levels…the usual!
#Conservators At Work 💡at the @fitzmuseum_uk! . Here Christine Kimbriel, Painting Conservator at the Hamilton-Kerr Institute, and 3rd year student Amiel Clarke (at the laptop), are carrying out analysis on Walter Sickert's Mornington Crescent Nude in Gallery 1, using portable #Xray fluorescence #spectrometry technique (#pXRF analysis). The instrument, which allows non-destructive analysis of the painting's surface, will aid with the identification of #pigments used by Sickert. This information will feed into Amiel's 3rd year project, investigating Sickert's painting techniques and material use. . . . . Courtesy #Fitzwilliam @CambridgeUniversity #conservation #science #technology #conservacion #conservator (at The Fitzwilliam Museum, Cambridge)
Sweet, sweet science!
Follow-up data collection starts tomorrow!
I'm geekily excited to do some more PXRF!!
I just did a rough total on my PXRF scans. If I didn't have access to a unit, the scans would have cost somewhere between $7,000 and $12,000.
Gulp.